苯甲酸-Alpha-13C合成路线 （共 27 条）
反应条件
in diethyl ether; hexane
T=20°C; 0.333333 h; Title compound not separated from byproducts;
参考文献
Anderson; Broughton
Synthesis, 2001 , # 16 p. 2379 - 2380
反应条件
1: in water
T=-271.82°C; IrradiationInert atmosphere;
2: With dihydrogen peroxide in water
pH=7.4; aq. phosphate bufferInert atmosphere;
参考文献
Lippert, Alexander R.; Keshari, Kayvan R.; Kurhanewicz, John; Chang, Christopher J.
Journal of the American Chemical Society, 2011 , vol. 133, # 11 p. 3776 - 3779
反应条件
1: With pyridine in benzene
T=20°C; Acylation; 20 h;
2: With triethylamine in diethyl ether
T=20°C; Hydrolysis; 60 h;
参考文献
Young, David J.; Robinson, Michael J.T.
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 2 p. 121 - 126
反应条件
magnesium
1) ether, 2) ether, 0 deg C, 70 min; Multistep reaction;
参考文献
Takeuchi, Ken'ichi; Murai, Osamu; Matsui, Shin; Inoue, Takeshi; Kitagawa, Toshikazu; Okamoto, Kunio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 9 p. 1301 - 1310
反应条件
in 1,2-dichloro-ethane
T=75°C;
参考文献
Okamoto, Kunio; Takeuchi, Ken'ichi; Murai, Osamu; Matsui, Shin; Inoue, Takeshi; Kitagawa, Toshikazu
Tetrahedron Letters, 1981 , vol. 22, # 29 p. 2785 - 2788
参考文献
Chaloner, Penny A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 1028 - 1032
反应条件
dihydrogen peroxide; ozone
1) aq. acetic acid, ethyl acetate, 0 deg C, 22 h, 2) aq. acetic acid, ethyl acetate, r. t., 12 h; Multistep reaction;
参考文献
Franke, Wilfried; Schwarz, Helmut; Thies, Helga; Chandrasekhar, Jayaraman; Raque' Schleyer, Paul von; et al.
Chemische Berichte, 1981 , vol. 114, # 8 p. 2808 - 2824
反应条件
in 1,2-dichloro-ethane
T=75°C; 51 h; Product distributionMechanism;
参考文献
Takeuchi, Ken'ichi; Murai, Osamu; Matsui, Shin; Inoue, Takeshi; Kitagawa, Toshikazu; Okamoto, Kunio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 9 p. 1301 - 1310
反应条件
methanesulfonic acid
5 h; Heating;
参考文献
Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gazzetto, Sonia
Journal of Organic Chemistry, 1997 , vol. 62, # 21 p. 7228 - 7233
反应条件
in methanol; diethyl ether; water
参考文献
Timm, Uwe; Merkle, Ursula; Meier, Herbert
Chemische Berichte, 1980 , vol. 113, # 7 p. 2519 - 2529
