3-硝基-4-氯苯甲酰氯合成路线 （共 35 条）
反应条件
thionyl chloride in dichloromethane; N,N-dimethyl-formamide Heating;
参考文献
Berrada, Amal; Cavelier, Florine; Jacquier, Robert; Verducci, Jean
Bulletin de la Societe Chimique de France, 1989 , # 4 p. 511 - 514
参考文献
Eli Lilly and Company
Patent: US4008243 A1, 1977 ;
反应条件
in 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran; N,N-dimethyl-formamide
参考文献
Zeneca Limited
Patent: US5451594 A1, 1995 ;
反应条件
1: oxalyl chloride; DMF / CH2Cl2 / 20 °C 2: HCl View Scheme
参考文献
Spiniello, Marisa; White, Jonathan M.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 17 p. 3094 - 3101
参考文献
Spiniello, Marisa; White, Jonathan M.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 17 p. 3094 - 3101
反应条件
1: bei der Nitrierung 2: PCl5 View Scheme
参考文献
Montagne
Recueil des Travaux Chimiques des Pays-Bas, 1900 , vol. 19, p. 55
反应条件
aluminium trichloride T=70 - 85°C;
参考文献
Parlow, John J.; Mischke, Deborah A.; Woodard, Scott S.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 5908 - 5919
反应条件
aluminium trichloride
参考文献
Kraynack, Erica A.; Dalgard, Jackline E.; Gaeta, Federico C. A.
Tetrahedron Letters, 1998 , vol. 39, # 42 p. 7679 - 7682
反应条件
1: tetrachloromethane; aqueous ammonia 2: phosphorus oxychloride / 170 °C View Scheme
参考文献
GLAXOSMITHKLINE LLC; HALLMAN, Jason; LAUDEMAN, Christopher; LIU, Ronggang; MILLER, Aaron; MOORE, Michael, Lee; DOCK, Steven; MUSSO, David; PARRISH, Cynthia
Patent: WO2011/56635 A1, 2011 ;
WO 2011/056635 A1
反应条件
pyridine in tetrahydrofuran Esterification;
参考文献
Um, Ik-Hwan; Lee, Ji-Youn; Fujio, Mizue; Tsuno, Yuho
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 15 p. 2979 - 2985
