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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
38821-25-9
合成路线
（共 10 条）
38821-25-9
→
反应条件
451-40-1
二苯基乙酮
反应条件
1: RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; hydrogen; potassium tert-butylate / isopropyl alcohol / 40 h / 25 °C / 5171.62 Torr / |Glovebox 2: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C 3: dimethylsulfoxide-d6 / 0.5 h 4: aq. buffer / 0.25 h / |Inert atmosphere; |Irradiation View Scheme
参考文献
Kulasekharan, Revathy; Maddipatla, Murthy V. S. N.; Parthasarathy, Anand; Ramamurthy
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 942 - 949
38821-25-9
→
反应条件
451-40-1
二苯基乙酮
反应条件
1: RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; hydrogen; potassium tert-butylate / isopropyl alcohol / 40 h / 25 °C / 5171.62 Torr / |Glovebox 2: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C 3: benzene / |Irradiation View Scheme
参考文献
Kulasekharan, Revathy; Maddipatla, Murthy V. S. N.; Parthasarathy, Anand; Ramamurthy
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 942 - 949
38821-25-9
→
反应条件
451-40-1
二苯基乙酮
+
64357-67-1
反应条件
2 h; Irradiationinclusion complex of zeolite LiX;
参考文献
Journal of Organic Chemistry, , vol. 55, # 18 p. 5269 - 5278
38821-25-9
→
反应条件
451-40-1
二苯基乙酮
+
64357-67-1
反应条件
in benzene 6 h; Irradiationother α-alkyldeoxybenzoins; reaction with zeolites as medium; Product distributionMechanism;
参考文献
Corbin, D. R.; Eaton, D. F.; Ramamurthy, V.
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5384 - 5386
38821-25-9
→
反应条件
451-40-1
二苯基乙酮
+
64357-67-1
+
115732-30-4
反应条件
2 h; Irradiationinclusion complex of various zeolites; comparison with photolysis in benzene; Product distributionMechanism;
参考文献
Ramamurthy, V.; Corbin, D. R.; Eaton, D. F.
Journal of Organic Chemistry, 1990 , vol. 55, # 18 p. 5269 - 5278
38821-25-9
→
反应条件
2042-85-5
1,2-二(苯基)丙-1-酮
反应条件
1.1: RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; hydrogen; potassium tert-butylate / isopropyl alcohol / 40 h / 25 °C / 5171.62 Torr / |Glovebox 2.1: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C 3.1: benzene / |Irradiation 4.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C 4.2: 2 h / 3 - 20 °C View Scheme
参考文献
Kulasekharan, Revathy; Maddipatla, Murthy V. S. N.; Parthasarathy, Anand; Ramamurthy
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 942 - 949
38821-25-9
→
反应条件
18220-90-1
4-乙基苯甲酮
反应条件
1.1: RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; hydrogen; potassium tert-butylate / isopropyl alcohol / 40 h / 25 °C / 5171.62 Torr / |Glovebox 2.1: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C 3.1: benzene / |Irradiation 4.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C 4.2: 2 h / 3 - 20 °C 5.1: RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; hydrogen; potassium tert-butylate / isopropyl alcohol / 40 h / 25 °C / 5171.62 Torr / |Glovebox 6.1: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C 7.1: dimethylsulfoxide-d6 / 0.5 h 8.1: aq. buffer / 0.25 h / |Inert atmosphere; |Irradiation View Scheme
参考文献
Kulasekharan, Revathy; Maddipatla, Murthy V. S. N.; Parthasarathy, Anand; Ramamurthy
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 942 - 949
38821-25-9
→
反应条件
451-40-1
二苯基乙酮
+
64357-67-1
反应条件
2 h; Irradiationinclusion complex of zeolite LiX;
参考文献
Ramamurthy, V.; Corbin, D. R.; Eaton, D. F.
Journal of Organic Chemistry, 1990 , vol. 55, # 18 p. 5269 - 5278
38821-25-9
→
反应条件
451-40-1
二苯基乙酮
+
64357-67-1
反应条件
in benzene 6 h; Irradiationother α-alkyldeoxybenzoins; reaction with zeolites as medium; Product distributionMechanism;
参考文献
Corbin, D. R.; Eaton, D. F.; Ramamurthy, V.
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5384 - 5386
38821-25-9
→
反应条件
451-40-1
二苯基乙酮
+
64357-67-1
+
115732-30-4
反应条件
2 h; Irradiationinclusion complex of various zeolites; comparison with photolysis in benzene; Product distributionMechanism;
参考文献
Ramamurthy, V.; Corbin, D. R.; Eaton, D. F.
Journal of Organic Chemistry, 1990 , vol. 55, # 18 p. 5269 - 5278
