反应条件
1: 72 percent / toluene-p-sulphonic acid / toluene / 24 h / Heating 2: 2.) 30percent sodium hydroxide / 1.) toluene, reflux, 2 d; 2.) water, reflux 2h 3: 41 percent / butyl-lithium / tetrahydrofuran / 1.) -78 degC, 4 h, 2.) -78 degC to R. T. 4: 85 percent / m-chloroperbenzoic acid / CHCl3 / 2 h / Ambient temperature 5: 95 percent / toluene / 6 h / 100 °C 6: 75 percent / 1.) butyl-lithium, 2.) benzaldehyde, H2O / tetrahydrofuran / 1.) -60 degC, 2.) -78 degC to R. T. View Scheme
参考文献
Cornish Christopher A.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2585 - 2598
