1: With [{(η5-C5Me5)IrCl}2(μ-Cl)2]; water in dichloromethane T=20°C; 24 h; Schlenk techniqueInert atmosphere; 2: With hydrogenchloride; water in acetonitrile-D3 T=20°C; 24 h; Schlenk techniqueInert atmosphereIrradiation;
参考文献
Journal of Organometallic Chemistry, , vol. 724, p. 275 - 280
1: With diethylaluminium chloride in dichloromethane T=-78°C; chelation; 0.5 h; 2: With tri-n-butyl-tin hydride T=-78°C; Reduction; 1 h; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 122, # 19 p. 4817 - 4818
