1,8-萘啶-2-羧酸乙酯合成路线 (共 2 条)
反应条件
piperidine; sodium sulfate; trifluoroacetic acid; copper(ll) bromide in 1,2-dichloro-ethane
1 h; Inert atmosphereReflux;
参考文献
Sakai, Norio; Tamura, Kosuke; Shimamura, Kazuyori; Ikeda, Reiko; Konakahara, Takeo
Organic Letters, 2012 , vol. 14, # 3 p. 836 - 839
反应条件
1: copper(l) iodide; Pd2(PPh3)2Cl2; diethylamine / 20 °C / Inert atmosphere
2: piperidine; sodium sulfate; trifluoroacetic acid; copper(ll) bromide / 1,2-dichloro-ethane / 1 h / Inert atmosphere; Reflux
View Scheme
参考文献
Sakai, Norio; Tamura, Kosuke; Shimamura, Kazuyori; Ikeda, Reiko; Konakahara, Takeo
Organic Letters, 2012 , vol. 14, # 3 p. 836 - 839