R(+)-alpha-甲基苄胺合成路线 (共 285 条)
反应条件
sulfuric acid in water 2 h; Ambient temperature; Yield given;
参考文献
Ikota; Achiwa; Yamada
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 887 - 894
反应条件
sulfuric acid in water 2 h; Ambient temperature; Yield given;
参考文献
Ikota; Achiwa; Yamada
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 887 - 894
反应条件
sulfuric acid in water 2 h; Ambient temperature; Yield given;
参考文献
Ikota; Achiwa; Yamada
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 887 - 894
反应条件
sulfuric acid in water 2 h; Ambient temperature; Yield given;
参考文献
Ikota; Achiwa; Yamada
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 887 - 894
反应条件
sulfuric acid in water 2 h; Ambient temperature; Yield given;
参考文献
Ikota; Achiwa; Yamada
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 887 - 894
反应条件
hydroxylammonium acetate in ethanol 10 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yuanwei, Chen; Aiqiao, Mi; Xun, Xiao; Yaozhong, Jiang
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1423 - 1430
反应条件
hydroxylammonium acetate in ethanol 10 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yuanwei, Chen; Aiqiao, Mi; Xun, Xiao; Yaozhong, Jiang
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1423 - 1430
反应条件
methanol; Amberlyst 15; ammonia 1.) CH2Cl2, 25 deg C, 12 h, 2.) 50 min; Yield given. Multistep reaction;
参考文献
Liu, Yun-Shan; Zhao, Cunxiang; Bergbreiter, David E.; Romo, Daniel
Journal of Organic Chemistry, 1998 , vol. 63, # 10 p. 3471 - 3473
反应条件
potassium hydroxide; potassium dihydrogenphosphate; Alcaligenes faecalis penicillin acylase in water T=25°C; pH=7.5; 5 h;
参考文献
Guranda, Dorel T.; Ushakov, Gennadij A.; Yolkin, Petr G.; Svedas, Vytas K.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 74, # 1-2 p. 48 - 53
反应条件
1: 1-amino-1-phenylethane With N,N'-dimethyl-N,N'-propyleneurea T=-20°C; 24 h; 2: C10H14N2O5S2F6 With N,N'-dimethyl-N,N'-propyleneurea T=-20°C; 24 h; Further stages.;
参考文献
Satyanarayana, Tummanapalli; Kagan, Henri B.
Tetrahedron, 2007 , vol. 63, # 28 p. 6415 - 6422