N n-二甲基-9-十八酰胺合成路线 （共 11 条）
反应条件
hydrogen; Cu-Ca oxides on zeolite with Cu/Ca=4:1 T=250°C; P=11251.1 Torr; Product distribution / selectivity;
参考文献
Kao Corporation
Patent: EP1992608 A1, 2008 ;
Location in patent: Page/Page column 10 ;
反应条件
LiAlH2(OEt)2 in diethyl ether
参考文献
Brown,H.C.; Tsukamoto,A.
Journal of the American Chemical Society, 1964 , vol. 86, p. 1089 - 1095
反应条件
hydrogen; sponge copper catalyst: 73.4percent Cu, 0.5percent Mg, 5.7percent Fe, 0.9percent Al in water T=250°C; P=11251.1 Torr; Inert atmosphereAutoclave;
参考文献
Kao Corporation
Patent: US2010/179349 A1, 2010 ;
Location in patent: Page/Page column 6 ;
反应条件
hydrogen; magnesium/copper (0.76 ratio) oxide catalyst with copper content 40percent by mass T=250°C; P=3750.38 Torr; 6 h; Autoclave; Product distribution / selectivity;
参考文献
EP2103594 A1, ;
Page/Page column 10 ;
反应条件
hydrogen; Cu-Ca oxides on zeolite with Cu/Ca=4:1 T=250°C; P=11251.1 Torr; Product distribution / selectivity;
参考文献
Kao Corporation
Patent: EP1992608 A1, 2008 ;
Location in patent: Page/Page column 10 ;
反应条件
hydrogen; magnesium/copper (0.76 ratio) oxide catalyst with copper content 40percent by mass T=250°C; P=3750.38 Torr; 6 h; Autoclave; Product distribution / selectivity;
参考文献
EP2103594 A1, ;
Page/Page column 10 ;
反应条件
hydrogen; Cu-Ca oxides on zeolite with Cu/Ca=4:1 T=250°C; P=11251.1 Torr; Product distribution / selectivity;
参考文献
Kao Corporation
Patent: EP1992608 A1, 2008 ;
Location in patent: Page/Page column 10 ;
反应条件
N-ethyl-N,N-diisopropylamine; [bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane
T=0°C; 0.5 h;
参考文献
Kangani, Cyrous O.; Kelley, David E.
Tetrahedron Letters, 2005 , vol. 46, # 51 p. 8917 - 8920
参考文献
Staudinger; Roessler
Chemische Berichte, 1936 , vol. 69, p. 50
反应条件
potassium hydroxide; bis(o-nitrophenyl)phenylphosphonate; 4 A molecular sieve; tetrabutylammomium bromide; triethylamine
1.) THF/water, 1 h, 2.) THF, RT, 2 h; Yield given. Multistep reaction;
参考文献
Watanabe, Yutaka; Mukaiyama, Teruaki
Chemistry Letters, 1981 , p. 285 - 288
