3-氨基-1-(3,4-二氯苯基)硫脲合成路线 (共 3 条)
反应条件
hydrazine hydrate in isopropyl alcohol
T=20°C; 3 h; Inert atmosphere;
参考文献
Serra, Silvia; Moineaux, Laurence; Vancraeynest, Christelle; Masereel, Bernard; Wouters, Johan; Pochet, Lionel; Frederick, Raphael
European Journal of Medicinal Chemistry, 2014 , vol. 82, p. 96 - 105
反应条件
hydrazine hydrate in ethanol
T=20°C; 0.25 h;
参考文献
El-Sharief, Ahmed M. Sh.; Moussa, Ziad
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 11 p. 4315 - 4334
反应条件
1: With ammonia in ethanol; water
0.75 h;
2: With sodium carbonate; chloroacetic acid in ethanol; water
3: With hydrazine in ethanol; water
0.75 h; Reflux;
参考文献
Pareek, Alok K.; Joseph; Seth, Daya S.
Oriental Journal of Chemistry, 2010 , vol. 26, # 4 p. 1549 - 1552