2,2-二甲基乙酰乙酸甲酯合成路线 （共 44 条）
反应条件
1: 1.) t-AmONa / 1.) benzene, 25 deg C, 3 h, 2.) 12 h 2: 90 percent / red HgO, BF3*Et2O / tetrahydrofuran; H2O / 0.42 h / Ambient temperature 3: NaOMe / methanol / 2 h / Ambient temperature View Scheme
参考文献
Kende, Andrew S.; Becker, David A.
Synthetic Communications, 1982 , vol. 12, # 11 p. 829 - 832
反应条件
sodium methylate in methanol 2 h; Ambient temperature;
参考文献
Kende, Andrew S.; Becker, David A.
Synthetic Communications, 1982 , vol. 12, # 11 p. 829 - 832
反应条件
in tetrahydrofuran Ambient temperature;
参考文献
Bourgeois, M. J.; Montaudon, E.; Campagnole, M.; Maillard, B.
Bulletin des Societes Chimiques Belges, 1982 , vol. 91, # 10 p. 871 - 872
反应条件
potassium carbonate T=0°C; 2.16667 h; Title compound not separated from byproducts;
参考文献
Collins, David J.; Choo, Gabrielyn Lee Poh; Obrist, Hans
Australian Journal of Chemistry, 1990 , vol. 43, # 3 p. 617 - 622
参考文献
Saito,K.; Sato,T.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, p. 3601 - 3605
参考文献
Bruehl
Journal fuer Praktische Chemie (Leipzig), 1894 , vol. <2> 50, p. 137
Chemische Berichte, 1902 , vol. 35, p. 3619
参考文献
Bruehl
Journal fuer Praktische Chemie (Leipzig), 1894 , vol. <2> 50, p. 137
Chemische Berichte, 1902 , vol. 35, p. 3619
反应条件
bei 8-stdg.Kochen und Zersetzung des Reaktionsprodukts mit warmer verduennter Salzsaeure;
参考文献
Robinson
Journal of the Chemical Society, 1916 , vol. 109, p. 1045
参考文献
Perkin
Journal of the Chemical Society, 1903 , vol. 83, p. 1249
反应条件
1: LDA / tetrahydrofuran / -78 deg C to RT 2: Ph3P, NEt3, HCO2H / Pd(OAc)2 / dimethylformamide / 2068.6 Torr / Ambient temperature View Scheme
参考文献
Freskos; Laneman; Reilly; Ripin
Tetrahedron Letters, 1994 , vol. 35, # 6 p. 835 - 838
