2-氯-N-(2-苯基乙基)苯甲酰胺合成路线 （共 6 条）
反应条件
phosphorus pentoxide in xylene Dehydration; cyclization; Heating;
参考文献
Suna; Trapencieris
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 3 p. 287 - 300
反应条件
triethylamine in dichloromethane
T=20°C; 3 h;
参考文献
Yang, Jie; Hua, Wei-Yi; Wang, Fu-Xiang; Wang, Zhi-Yuan; Wang, Xiang
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 24 p. 6547 - 6557
反应条件
tert.-butylhydroperoxide; manganese(IV) oxide in water; acetonitrile
T=80°C; 48 h;
参考文献
Vanjari, Rajeshwer; Guntreddi, Tirumaleswararao; Singh, Krishna Nand
Organic Letters, 2013 , vol. 15, # 18 p. 4908 - 4911
反应条件
1: N-chloro-succinimide / acetonitrile / 3 h / 20 °C
2: tert.-butylhydroperoxide; manganese(IV) oxide / water; acetonitrile / 48 h / 80 °C
View Scheme
参考文献
Vanjari, Rajeshwer; Guntreddi, Tirumaleswararao; Singh, Krishna Nand
Organic Letters, 2013 , vol. 15, # 18 p. 4908 - 4911
反应条件
1: thionyl chloride / CH2Cl2 / 0 - 20 °C
2: 92.9 percent / triethylamine / CH2Cl2 / 3 h / 20 °C
View Scheme
参考文献
Yang, Jie; Hua, Wei-Yi; Wang, Fu-Xiang; Wang, Zhi-Yuan; Wang, Xiang
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 24 p. 6547 - 6557
反应条件
1: POCl3 / acetonitrile / 3 h / Heating
2: 72 percent / MnO2 / benzene / 96 h / Heating
View Scheme
参考文献
Janin, Yves L.; Roulland, Emmanuel; Beurdeley-Thomas, Arnaud; Decaudin, Didier; Monneret, Claude; Poupon, Marie-France
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 529 - 532
