3,3-二甲基-2-氧代丁酸甲酯合成路线 （共 8 条）
反应条件
1: diethyl ether 3: phosphoric acid / 150 - 160 °C View Scheme
参考文献
Richard
Annales de Chimie (Cachan, France), 1910 , vol. <8> 21, p. 394
反应条件
mercury(II) diacetate in acetic acid
Ambient temperature;
参考文献
Gassmann, J.; Guenther, H.; Osternack, K.; Sawluk, A.; Thimm, K.; Voss, J.
Magnetic Resonance in Chemistry, 1994 , vol. 32, # 10 p. 624 - 630
反应条件
Amberlite H+ ion exchange resin IR-120 HPC; water in methanol
Heating;
参考文献
Katritzky, Alan R.; Wang, Zuoquan; Wells, Adam P.; Steel, Peter J.
Organic Preparations and Procedures International, 1995 , vol. 27, # 4 p. 457 - 462
反应条件
Coprinus peroxidase; 2-methoxy-phenol in water
T=20°C; 336 h; pH 7.0;
参考文献
Adam, Waldemar; Mock-Knoblauch, Cordula; Saha-Moeller, Chantu R.
Journal of Organic Chemistry, 1999 , vol. 64, # 13 p. 4834 - 4839
反应条件
(i) KMnO4, aq. NaOH, (ii) (methylation); Multistep reaction;
参考文献
Dubois,J.E.; Bauer,P.
Journal of the American Chemical Society, 1976 , vol. 98, # 22 p. 6993 - 6999
反应条件
(i) KMnO4, aq. NaOH, (ii) /BRN= 1098229/, H2SO4; Multistep reaction;
参考文献
Bauer,P.; Dubois,J.E.
Journal of the American Chemical Society, 1976 , vol. 98, # 22 p. 6999 - 7007
反应条件
1: 80 percent / butyl-lithium, chlorotrimethylsilane / hexane; tetrahydrofuran / 1 h / 0 °C
2: 90 percent Chromat. / NaBH3CN / methanol / 0.25 h / Ambient temperature
View Scheme
参考文献
Matsuda, Yoshihiko; Tanimoto, Shigeo; Okamoto, Tadashi; Ali, Syed Mashhood
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 279 - 281
反应条件
1: diethyl ether
3: KMnO4 / in alkal. Loesung
View Scheme
参考文献
Richard
Annales de Chimie (Cachan, France), 1910 , vol. <8> 21, p. 394
