4-叔-丁基-2-氟-苯酚合成路线 (共 19 条)
反应条件
CsSO4F in acetonitrile
1 h; Ambient temperature;
参考文献
Stavber; Zupan
Tetrahedron, 1992 , vol. 48, # 28 p. 5875 - 5882
反应条件
CsSO4F in acetonitrile
1 h; Ambient temperature;
参考文献
Stavber; Zupan
Tetrahedron, 1992 , vol. 48, # 28 p. 5875 - 5882
反应条件
CsSO4F in acetonitrile
1 h; Ambient temperature; Yield given;
参考文献
Stavber; Zupan
Tetrahedron, 1992 , vol. 48, # 28 p. 5875 - 5882
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in methanol
5 h; Heating;
参考文献
Zupan, Marko; Iskra, Jernej; Stavber, Stojan
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 6 p. 1655 - 1660
反应条件
aluminium trichloride
24 h; Ambient temperature;
参考文献
Tashiro, Masashi; Yoshiya, Haruo; Fukata, Gouki
Journal of Organic Chemistry, 1981 , vol. 46, # 19 p. 3784 - 3789
反应条件
1.1: 3,4,5,6-tetrachloro-1,2-benzoquinone / chloroform / 0 - 20 °C / Inert atmosphere
2.1: [bis(2-methoxyethyl)amino]-sulfur trifluoride / chloroform / 0 - 20 °C / Inert atmosphere
2.2: 0 - 50 °C
View Scheme
参考文献
Nemoto, Hiroyuki; Nishiyama, Tsuyoshi; Akai, Shuji
Organic Letters, 2011 , vol. 13, # 10 p. 2714 - 2717
反应条件
CsSO4F; ethyl iodide
1) MeCN, r.t., 1 h, 2) r.t., 1 h; Yield given. Multistep reaction;
参考文献
Stavber; Zupan
Tetrahedron, 1992 , vol. 48, # 28 p. 5875 - 5882
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate)
T=70°C; 24 h; Ionic liquid;
参考文献
Pavlinac, Jasminka; Zupan, Marko; Stavber, Stojan
Molecules, 2009 , vol. 14, # 7 p. 2394 - 2409
反应条件
accufluorTM in acetonitrile
T=20°C; 24 h; Product distribution; Further Variations:ReagentsSolventsTemperaturesreaction time;
参考文献
Pravst, Igor; Iskra, Maja Papez; Jereb, Marjan; Zupan, Marko; Stavber, Stojan
Tetrahedron, 2006 , vol. 62, # 18 p. 4474 - 4481