Resveratroloside合成路线 (共 13 条)
反应条件
sodium hydroxide in tetrahydrofuran; methanol T=0 - 25°C; 5 h;
参考文献
Zhang, Zhaojun; Yu, Biao; Schmidt, Richard R.
Synthesis, 2006 , # 8 p. 1301 - 1306
反应条件
sodium methylate in methanol T=20°C; 1 h;
参考文献
Learmonth, David A.
Synthetic Communications, 2004 , vol. 34, # 9 p. 1565 - 1575
反应条件
catharanthus roseus in methanol T=25°C; 120 h; Microbiological reaction;
参考文献
Imai, Hiroya; Kitagawa, Megumi; Ishihara, Kohji; Masuoka, Noriyoshi; Shimoda, Kei; Nakajima, Nobuyoshi; Hamada, Hiroki
Bioscience, Biotechnology and Biochemistry, 2012 , vol. 76, # 8 p. 1552 - 1554
反应条件
glucosyltransferase OleD ASP in dimethyl sulfoxide T=20°C; pH=8; 3 h; Enzymatic reaction; TemperatureSolvent;
参考文献
Zhou, Maoquan; Hamza, Adel; Zhan, Chang-Guo; Thorson, Jon S.
Journal of Natural Products, 2013 , vol. 76, # 2 p. 279 - 286
反应条件
1: 80 percent / 4 Angstroem molecular sieves; trimethylsilyl triflate / CH2Cl2 / 5 h / 0 - 25 °C 2: 95 percent / aq. NaOH / methanol; tetrahydrofuran / 5 h / 0 - 25 °C View Scheme
参考文献
Zhang, Zhaojun; Yu, Biao; Schmidt, Richard R.
Synthesis, 2006 , # 8 p. 1301 - 1306
反应条件
1: 10 percent / imidazole / dimethylformamide / 6 h / -5 - 20 °C 2: 80 percent / 4 Angstroem molecular sieves; trimethylsilyl triflate / CH2Cl2 / 5 h / 0 - 25 °C 3: 95 percent / aq. NaOH / methanol; tetrahydrofuran / 5 h / 0 - 25 °C View Scheme
参考文献
Zhang, Zhaojun; Yu, Biao; Schmidt, Richard R.
Synthesis, 2006 , # 8 p. 1301 - 1306
反应条件
1: 61 percent / Pd(OAc02; benzyltriethylammonium chloride; Bu3N / acetonitrile / 2 h / 100 °C 2: 97 percent / NaOMe / methanol / 1 h / 20 °C View Scheme
参考文献
Learmonth, David A.
Synthetic Communications, 2004 , vol. 34, # 9 p. 1565 - 1575
反应条件
1: 30 percent / Ag2CO3 / acetonitrile / 48 h / 20 °C 2: 61 percent / Pd(OAc02; benzyltriethylammonium chloride; Bu3N / acetonitrile / 2 h / 100 °C 3: 97 percent / NaOMe / methanol / 1 h / 20 °C View Scheme
参考文献
Learmonth, David A.
Synthetic Communications, 2004 , vol. 34, # 9 p. 1565 - 1575
反应条件
1: 61 percent / Pd(OAc02; benzyltriethylammonium chloride; Bu3N / acetonitrile / 2 h / 100 °C 2: 97 percent / NaOMe / methanol / 1 h / 20 °C View Scheme
参考文献
Learmonth, David A.
Synthetic Communications, 2004 , vol. 34, # 9 p. 1565 - 1575
反应条件
1: 30 percent / Ag2CO3 / acetonitrile / 48 h / 20 °C 2: 61 percent / Pd(OAc02; benzyltriethylammonium chloride; Bu3N / acetonitrile / 2 h / 100 °C 3: 97 percent / NaOMe / methanol / 1 h / 20 °C View Scheme
参考文献
Learmonth, David A.
Synthetic Communications, 2004 , vol. 34, # 9 p. 1565 - 1575