2-乙酰基戊-4-烯酸甲酯合成路线 (共 19 条)
反应条件
phenolated sodium; palladium
参考文献
Takahashi,K. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 230 - 236
反应条件
trans-Mo(N2)2(1,2-bis(diphenylphosphino)ethane)2
T=150°C; 4 h;
参考文献
Tatsumi, T.; Hashimoto, K.; Tominaga, H.; Mizuta, Y.; Hata, K.; et al.
Journal of Organometallic Chemistry, 1983 , vol. 252, # 1 p. 105 - 112
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in benzene
3 h; Ambient temperature;
参考文献
Nakamura, Kaoru; Miyai, Takehiko; Nagar, Ashish; Oka, Shinzaburo; Ohno, Atsuyoshi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 4 p. 1179 - 1187
反应条件
Ni(1,4-bis(diphenylphosphanyl)butane)2 in N,N-dimethyl-formamide
T=80°C; 0.1 h; other catalysts, solvents and times; Product distribution;
参考文献
Bricout, Herve; Carpentier, Jean-Francois; Mortreux, Andre
Chemical Communications, 1997 , # 15 p. 1393 - 1394
反应条件
polypyrrole supported phosphine borane complex (3 molpercent); sodium hydride; palladium diacetate
1.) THF, r.t., 30 min, r.t., 15 min; 2.) THF, r.t., 30 min, r.t., 62 h; Yield given. Multistep reaction;
参考文献
Riegel, Nadege; Darcel, Christophe; Stephan, Olivier; Juge, Sylvain
Journal of Organometallic Chemistry, 1998 , vol. 567, # 1-2 p. 219 - 233
反应条件
1-methyl-piperidine; [Ru(η4-C8H12)(η6-C8H10)]
T=50°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zhang, Shi-Wei; Mitsudo, Take-aki; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1993 , vol. 450, # 1.2 p. 197 - 207
反应条件
sodium hydride in benzene
0.5 h; Heating; Yield given. Yields of byproduct given;
参考文献
Keinan, Ehud; Sinha, Subhash C.; Sinha-Bagchi, Anjana
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3333 - 3340
反应条件
polypyrrole supported phosphine borane complex (6.4 molpercent); sodium hydride; palladium diacetate in tetrahydrofuran
48 h; Ambient temperaturevarious borane complexes; Product distribution;
参考文献
Riegel, Nadege; Darcel, Christophe; Stephan, Olivier; Juge, Sylvain
Journal of Organometallic Chemistry, 1998 , vol. 567, # 1-2 p. 219 - 233
参考文献
Kazankova,M.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, # 8 p. 1447 - 1453,1450 - 1455