N-(2-羟基-苯基)-4-甲基-苯磺酰胺合成路线 （共 18 条）
反应条件
1: 94 percent / Et3N / CH2Cl2 / 1 h / Ambient temperature
2: 95 percent / n-BuLi / diethyl ether; hexane / 1 h / Ambient temperature
View Scheme
参考文献
Andersen, Kenneth K.; Gowda, Gopala; Jewell, Linda; McGraw, Phillip; Phillips, Brian T.
Journal of Organic Chemistry, 1982 , vol. 47, # 10 p. 1884 - 1889
反应条件
1: 97 percent / NaH / 1 h
2: 96 percent / Br2 / CH2Cl2 / 20 °C
3: 95 percent / LiOH / methanol
4: NaH / tetrahydrofuran / 20 °C
View Scheme
参考文献
Cabanal-Duvillard, Isabelle; Berrien, Jean-Francois; Royer, Jacques; Husson, Henri-Philippe
Tetrahedron Letters, 1998 , vol. 39, # 29 p. 5181 - 5184
反应条件
hydrogenchloride; sodium methylate
1) CH3CN, room temperature, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Andersen, Kenneth K.; Bray, Diana D.; Chumpradit, Sumalee; Clark, Michael E.; Habgood, Gregory J.; et al.
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6508 - 6516
反应条件
sulfuric acid
T=50°C; Kinetics; Further Variations:TemperaturesReagents;
参考文献
Bekdemir, Yunus; Kutuk, Halil; Celik, Sibel; Tillett, John G.
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 4 p. 973 - 980
参考文献
Bell
Journal of the Chemical Society, 1930 , p. 1981,1984
参考文献
Bell
Journal of the Chemical Society, 1930 , p. 1981,1984
参考文献
Bell
Journal of the Chemical Society, 1930 , p. 1981,1984
参考文献
Raiford; Shelton
Journal of Organic Chemistry, 1939 , vol. 4, p. 207,215
