2-甲基-2-壬基-1,3-二氧戊环合成路线 (共 2 条)
反应条件
dimethylboron bromide in dichloromethane; 1,2-dichloro-ethane T=-78°C; 1 h; diphenylboron bromide instead of dimethylboron bromide;
参考文献
Quindon, Yvan; Morton, Howard E.; Yoakim, Christiane
Tetrahedron Letters, 1983 , vol. 24, # 37 p. 3969 - 3972
反应条件
1: With toluene-4-sulfonic acid in toluene
3 h; Reflux;
2: With sodium hydroxide in water; toluene
参考文献
Dow Global Technologies LLC; TULCHINSKY, Michael, L.; BRIGGS, John, R.; RAND, Cynthia, L.
Patent: EP2318346 B1, 2013 ;
Location in patent: Paragraph 0075 ;