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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3899-91-0
合成路线
（共 45 条）
3899-91-0
+
36800-95-0
+
98-80-6
苯硼酸
→
反应条件
2920-38-9
4-氰基联苯
+
613-37-6
4-甲氧基联苯
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; (9-phenanthrenyl)Ni(II)(PPh3)2Cl; potassium carbonate in toluene T=110°C; Suzuki Coupling; 30 h; Inert atmosphere;
参考文献
Hu, Feng; Lei, Xiangyang
Tetrahedron, 2014 , vol. 70, # 25 p. 3854 - 3858
3899-91-0
→
反应条件
25245-35-6
2-碘-1,4-二甲氧基苯
反应条件
1: AcOH; I2; HIO3 / H2SO4 / CCl4 / 48 h / Heating 2: aq. NaOH / 2-methyl-propan-2-ol / 6 h / Heating 3: K2CO3 / acetone / 12 h / Heating View Scheme
参考文献
Yamaguchi, Yoshihiro; Tanaka, Takahiro; Kobayashi, Shigeya; Wakamiya, Tateaki; Matsubara, Yoshio; Yoshida, Zen-Ichi
Journal of the American Chemical Society, 2005 , vol. 127, # 26 p. 9332 - 9333
3899-91-0
+
99768-12-4
4-甲氧羰基苯硼酸
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; (9-phenanthrenyl)Ni(II)(PPh3)2Cl; potassium carbonate in toluene T=110°C; Suzuki Coupling; 30 h; Inert atmosphere; Reagent/catalyst;
参考文献
Hu, Feng; Lei, Xiangyang
Tetrahedron, 2014 , vol. 70, # 25 p. 3854 - 3858
3899-91-0
+
98-80-6
苯硼酸
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; (9-phenanthrenyl)Ni(II)(PPh3)2Cl; potassium carbonate in toluene T=110°C; Suzuki Coupling; 30 h; Inert atmosphere; Reagent/catalystSolventTimeConcentrationTemperature;
参考文献
Hu, Feng; Lei, Xiangyang
Tetrahedron, 2014 , vol. 70, # 25 p. 3854 - 3858
3899-91-0
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
potassium hydroxide; palladium diacetate in methanol T=60°C; Suzuki-Miyaura cross-coupling;
参考文献
Zhang, Liang; Meng, Tianhao; Wu, Jie
Journal of Organic Chemistry, 2007 , vol. 72, # 24 p. 9346 - 9349
3899-91-0
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
NiCl2((PPh3)P)2; caesium carbonate; triphenylphosphine; zinc; tri-cyclo-hexyl-phosphine in N,N-dimethyl-formamide; acetone T=20 - 80°C; Suzuki-Miyaura cross-coupling reaction; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Chemical Communications, , vol. 47, # 1 p. 307 - 309
3899-91-0
+
100-58-3
溴化苯基镁
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
1: phenyl-magnesium bromide With C24H52Cl2O12P4Pd2 in tetrahydrofuran; 1,4-dioxane T=20°C; Kumada-Corriu cross-coupling reaction; 0.0833333 h; Inert atmosphere; 2: para-methoxyphenyl tosylate in tetrahydrofuran; 1,4-dioxane T=80°C; Kumada-Corriu cross-coupling reaction; 24 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Kapdi, Anant R.; Fenner, Sabine; Kornhaab, Christoph; Schulzke, Carola
Chemistry - A European Journal, 2011 , vol. 17, # 10 p. 2965 - 2971
3899-91-0
+
100-59-4
苯基氯化镁
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
[Pd(dibenzylideneacetone)2] in tetrahydrofuran Kumada cross-coupling reaction; 22 h;
参考文献
Ackermann, Lutz; Althammer, Andreas
Organic Letters, 2006 , vol. 8, # 16 p. 3457 - 3460
3899-91-0
+
368-47-8
苯基三氟硅烷
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol T=60°C; Hiyama cross-coupling reaction; Inert atmosphere;
参考文献
Molander, Gary A.; Iannazzo, Laura
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 9182 - 9187
3899-91-0
+
36800-95-0
+
98-80-6
苯硼酸
→
反应条件
2920-38-9
4-氰基联苯
+
613-37-6
4-甲氧基联苯
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; (9-phenanthrenyl)Ni(II)(PPh3)2Cl; potassium carbonate in toluene T=110°C; Suzuki Coupling; 30 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 70, # 25 p. 3854 - 3858
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