in not given
ligand was condensed with Bu(t)C6H3(CN)2 and Zn at 213°C for 4 h; washed with hot H2O, dried, chromd. on a silica gel column, eluted with toluene and acetone, purified by h.p.l.c. with toluene:acetone, retention time: 3 min 40 s;
参考文献
Gaspard; Giannotti; Maillard; et al.
Journal of the Chemical Society - Series Chemical Communications, 1986 , vol. No. 16, p. 1239 - 1241