1-甲基-1氢-5-醛基-咪唑合成路线 （共 26 条）
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Tanaka, Akira; Ryuno, Aya; Okada, Saori; Satake, Akiharu; Kobuke, Yoshiaki
Israel Journal of Chemistry, 2005 , vol. 45, # 3 p. 281 - 291
反应条件
1: pyridine 2: Na2CO3; glycerol / 170 °C View Scheme
参考文献
Jones; McLaughlin
Journal of the American Chemical Society, 1949 , vol. 71, p. 2444,2447
反应条件
2: pyridine 3: Na2CO3; glycerol / 170 °C View Scheme
参考文献
Jones; McLaughlin
Journal of the American Chemical Society, 1949 , vol. 71, p. 2444,2447
反应条件
1: 62 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating 2: 95 percent / MnO2 / CHCl3 / 23 h / Heating View Scheme
参考文献
Dener, Jeffrey M.; Zhang, Lin-Hua; Rapoport, Henry
Journal of Organic Chemistry, 1993 , vol. 58, # 5 p. 1159 - 1166
参考文献
Sakami; Wilson
Journal of Biological Chemistry, 1944 , vol. 154, p. 215,219
反应条件
n-butyllithium 1.) THF, LiBr, -70 deg C, 2.) -70 deg C; Yield given. Multistep reaction;
参考文献
Shapiro, Gideon; Marzi, Martin
Tetrahedron Letters, 1993 , vol. 34, # 21 p. 3401 - 3404
反应条件
Behandeln des Reaktionsprodukts mit Soda;
参考文献
Hubball; Pyman
Journal of the Chemical Society, 1928 , p. 28
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 0.333333 h;
参考文献
YALE UNIVERSITY; UNIVERSITY OF SOUTH FLORIDA; UNIVERSITY OF WASHINGTON; SEBTI, Said
Patent: WO2006/102159 A2, 2006 ;
Location in patent: Page/Page column 22 ;
WO 2006/102159 A2
反应条件
1: (i) KOtBu, tBuOH, (ii) LiBH4, 1,2-dimethoxy-ethane, (iii) H2, PtO2-C, EtOH 2: KOtBu / butan-1-ol / Heating 3: (i) H2, PtO2-C, MeOH, (ii) Ac2O, AcOH, (iii) H2, PtO2, MeOH View Scheme
参考文献
Link,H.; Bernauer,K.
Helvetica Chimica Acta, 1972 , vol. 55, p. 1053 - 1062
反应条件
1: methanol; H2O / 20 °C 2: 16.3 g / NaBH4 / methanol; H2O View Scheme
参考文献
Collman, James P.; Zhong, Min; Costanzo, Simona; Zhang, Chi
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8252 - 8256
