1,4-二甲氧基-2,3-甲基苯合成路线 （共 18 条）
反应条件
N-bromosuccinmide in tetrachloromethane 1 h; Irradiationheating;
参考文献
Jansen; De Gelder; Rowan; Scheeren; Nolte
Journal of Organic Chemistry, 2001 , vol. 66, # 8 p. 2643 - 2653
反应条件
tetrachloromethane; N-bromosuccinmide; dibenzoyl peroxide
参考文献
McHale et al.
Journal of the Chemical Society, 1959 , p. 3358,3361
反应条件
bromine in chloroform T=20°C; 2 h;
参考文献
Sandulache, Angela; Silva, Artur M. S.; Cavaleiro, Jose A. S.
Monatshefte fur Chemie, 2003 , vol. 134, # 4 p. 551 - 563
反应条件
1: 91 percent / 60percent H2SO4 / 24 h / 40 °C 2: 88 percent / N-bromosuccinimide / CCl4 / 1 h / Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 120, # 15 p. 3650 - 3656
反应条件
sodium hydroxide in ethanol
Methylation; 3.5 h;
参考文献
Boufatah, Narimene; Gellis, Armand; Maldonado, Jose; Vanelle, Patrice
Tetrahedron, 2004 , vol. 60, # 41 p. 9131 - 9137
反应条件
potassium hydroxide in dimethyl sulfoxide
参考文献
Kotha, Sambasivarao; Kuki, Atsuo
Chemistry Letters, 1993 , # 2 p. 299 - 302
反应条件
copper(l) iodide; sodium methylate in N,N-dimethyl-formamide
Substitution; 24 h; Heating;
参考文献
Eskildsen, Jorgen; Christensen, Trine; Reenberg, Theis; Larsen, Uffe; Christensen, Jorn B.
Organic Preparations and Procedures International, 2000 , vol. 32, # 4 p. 398 - 400
反应条件
1: 84 percent / aq. NaOH
2: 91 percent / Br2 / acetic acid
3: 90 percent / NaOMe; CuI / dimethylformamide / 24 h / Heating
View Scheme
参考文献
Eskildsen, Jorgen; Christensen, Trine; Reenberg, Theis; Larsen, Uffe; Christensen, Jorn B.
Organic Preparations and Procedures International, 2000 , vol. 32, # 4 p. 398 - 400
反应条件
1: 91 percent / Br2 / acetic acid
2: 90 percent / NaOMe; CuI / dimethylformamide / 24 h / Heating
View Scheme
参考文献
Eskildsen, Jorgen; Christensen, Trine; Reenberg, Theis; Larsen, Uffe; Christensen, Jorn B.
Organic Preparations and Procedures International, 2000 , vol. 32, # 4 p. 398 - 400
反应条件
potassium carbonate; acetone; methyl iodide
参考文献
McHale et al.
Journal of the Chemical Society, 1959 , p. 3358,3361
