in benzene (Ar); standard Schlenk technique; mixt. of Pt compd. and B compd. in C6H6 was stirred for 3 h; volatiles removed (vac.); extd. (toluene); concd.; crystd. at -5°C; elem. anal.;
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diethylphosphoric acid ethyl ester in cyclohexane
Kinetics; 87°C, in a tube sealed under vac.; not sepd., detected by NMR;
参考文献
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triethylamine in tetrahydrofuran
byproducts: SiH(CH3)2Cl; bubbling H2 through THF soln. of platinum compd. and triethylamine for 20 min, addn. of phosphine deriv.; drying in vac.;
参考文献
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