反应条件
1.1: 88 percent / aq. KOH / 1 h / Heating
2.1: n-BuLi / tetrahydrofuran / -78 °C
2.2: B(OMe)3 / tetrahydrofuran / -78 - 20 °C
3.1: 100 percent / aq. Na2CO3 / Pd(PPh3)4 / 1,2-dimethoxy-ethane; ethanol / 42 h / Heating
4.1: 81 percent / aq. CAN / acetonitrile / 0.08 h / 20 °C
View Scheme
参考文献
Pathak, Rakhi; Vandayar, Kantharuby; Van Otterlo, Willem A. L.; Michael, Joseph P.; Fernandes, Manuel A.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3504 - 3509
