2-萘基(4-甲氧基苯基)甲酮合成路线 (共 17 条)
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
反应条件
ytterbium(III) triflate in nitromethane; methoxybenzene
参考文献
Kirin Beer Kabushiki Kaisha
Patent: US6143764 A1, 2000 ;
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane
T=100°C; P=760 Torr; 5 h;
参考文献
Andrus, Merritt B.; Ma, Yudao; Zang, Yunfu; Song, Chun
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9137 - 9140
反应条件
3,3-dimethyl-butan-2-one; [Ru(CO)3Cl2]2; K3PO4*3H2O; [(t-Bu)3PH]BF4 in water; toluene
T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Hong; Xu, Yuan; Shi, Erbo; Wei, Wei; Suo, Xiangqiang; Wan, Xiaobing
Chemical Communications, 2011 , vol. 47, # 27 p. 7880 - 7882
反应条件
bis(dibenzylideneacetone)-palladium(0) in toluene
T=23°C; Fukuyama reaction; Inert atmosphere;
参考文献
Kunchithapatham, Kamala; Eichman, Chad C.; Stambuli, James P.
Chemical Communications, 2011 , vol. 47, # 47 p. 12679 - 12681
反应条件
1: With N-iodo-succinimide; N-hexadecyl-N,N,N-trimethylammonium bromide; acetic acid in 1,4-dioxane; water
T=20°C;
2: in 1,4-dioxane; water
T=115°C; 0.25 h; Microwave irradiation;
3: With tert.-butylhydroperoxide; dipyridinium dichromate in 1,4-dioxane; water
T=115°C; 0.25 h; Microwave irradiation;
参考文献
Sharma, Naina; Sharma, Abhishek; Kumar, Rakesh; Shard, Amit; Sinha, Arun K.
European Journal of Organic Chemistry, 2010 , # 31 p. 6025 - 6032
反应条件
3,3-dimethyl-butan-2-one; [Ru(CO)3Cl2]2; K3PO4*3H2O; tri-cyclo-hexyl-phosphine in water; toluene
T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Hong; Xu, Yuan; Shi, Erbo; Wei, Wei; Suo, Xiangqiang; Wan, Xiaobing
Chemical Communications, 2011 , vol. 47, # 27 p. 7880 - 7882
反应条件
in diethyl ether
T=20°C; 20 h;
参考文献
Utley, James H.P; Rozenberg, Gregor G
Tetrahedron, 2002 , vol. 58, # 26 p. 5251 - 5265
反应条件
1: AlCl3; 1,1,2,2-tetrachloro-ethane
View Scheme
参考文献
Peck
Journal of the American Chemical Society, 1956 , vol. 78, p. 997,1000
反应条件
[Ru(CO)3Cl2]2; K3PO4*3H2O; [(t-Bu)3PH]BF4 in water; toluene
T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Hong; Xu, Yuan; Shi, Erbo; Wei, Wei; Suo, Xiangqiang; Wan, Xiaobing
Chemical Communications, 2011 , vol. 47, # 27 p. 7880 - 7882