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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
39077-95-7
合成路线
（共 6 条）
591-50-4
碘苯
+
39077-95-7
→
反应条件
831-91-4
苄基苯基硫醚
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; palladium diacetate; triphenylphosphine in 1,4-dioxane T=100°C; sulfenylation; 11 h;
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
696-62-8
4-碘苯甲醚
+
39077-95-7
→
反应条件
831-91-4
苄基苯基硫醚
+
26905-24-8
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; palladium diacetate; triphenylphosphine in 1,4-dioxane T=100°C; sulfenylation; 16 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 70, # 2 p. 445 - 456
2065-66-9
甲基三苯基碘化膦
+
39077-95-7
→
反应条件
831-91-4
苄基苯基硫醚
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane Arylation; 15 h; Heating;
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
696-62-8
4-碘苯甲醚
+
39077-95-7
→
反应条件
831-91-4
苄基苯基硫醚
+
26905-24-8
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; palladium diacetate; triphenylphosphine in 1,4-dioxane T=100°C; sulfenylation; 16 h;
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
636-98-6
4-硝基碘苯
+
39077-95-7
→
反应条件
27691-43-6
1-(苄基磺酰基)-4-硝基苯
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; palladium diacetate; triphenylphosphine in 1,4-dioxane T=100°C; sulfenylation; 6 h;
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
624-31-7
4-碘甲苯
+
39077-95-7
→
反应条件
5023-60-9
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; palladium diacetate; triphenylphosphine in 1,4-dioxane T=100°C; sulfenylation; 19 h;
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
