in tetrahydrofuran adding MeSSiMe3 to suspn. of (Cp*RuCl2)2 in THF, stirring at room temp. for 24 h; filtering pptd. solid off, washing with n-hexane, recrystn. from CH2Cl2-n-hexane;
参考文献
Nishibayashi; Wakiji; Ishii; Uemura; Hidai
Journal of the American Chemical Society, 2001 , vol. 123, # 14 p. 3393 - 3394
in benzene 4.62 mmol Me3SiSMe added to 4.62 mmol of the Ga compound in benzene; stirring at room temp.; filtration; solvent removed in vac.; elem. anal. (Cl2GaSC2H5);
参考文献
Hoffmann, G. G.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 558, p. 160 - 170
