in dichloromethane
under inert gas; to the boron-compound was dropped Me3SiSMe; mixt. refluxed for 3 d; solvent and Me3SiCl were condensed in vacuo; distillation; elem. anal., mass spectroscopy;
参考文献
Noeth, Heinrich; Pommerening, Hans
Chemische Berichte, 1986 , vol. 119, # 7 p. 2261 - 2271
in benzene
under inert gas; 5.12 mmol Me3SiSMe added to 5.12 mmol of the Al compound in benzene; stirring for 2 h at room temp.; solvent removed in vac.; solid treated with a large excess of C2H5SH at room temp.; filtration, solvent removed in vac.; solid washed with n-pentane and dried in vac.; elem. anal.;
参考文献
Hoffmann, G. G.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 558, p. 160 - 170
in benzene
4.62 mmol Me3SiSMe added to 4.62 mmol of the Ga compound in benzene; stirring at room temp.; filtration; solvent removed in vac.; elem. anal. (Cl2GaSC2H5);
参考文献
Hoffmann, G. G.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 558, p. 160 - 170
