1-(4-甲氧基苯基)-2-(4-硝基苯基)-乙炔合成路线 （共 24 条）
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate in 1,4-dioxane; water
T=23 - 60°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Struble, Justin R.; Lee, Suk Joong; Burke, Martin D.
Tetrahedron, 2010 , vol. 66, # 26 p. 4710 - 4718
反应条件
potassium tert-butylate in tert-butyl alcohol
T=50°C; 5 h;
参考文献
Pati, Hari N.; Wicks, Martha; Holt Jr., Herman L.; LeBlanc, Regan; Weisbruch, Paul; Forrest, Lori; Lee, Moses
Heterocyclic Communications, 2005 , vol. 11, # 2 p. 117 - 120
反应条件
potassium carbonate; 1,3-diphenyl-1,3-propanedione; copper(I) bromide; palladium dichloride in N,N-dimethyl-formamide
T=120°C; 20 h; Sealed tubeIn air;
参考文献
Pan, Delin; Zhang, Chun; Ding, Shengtao; Jiao, Ning
European Journal of Organic Chemistry, 2011 , # 25 p. 4751 - 4755
反应条件
caesium carbonate; bis(dibenzylideneacetone)-palladium(0) in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 12 h; Under air;
参考文献
Tang, Jian-Sheng; Tian, Mi; Sheng, Wen-Bing; Guo, Can-Cheng
Synthesis, 2012 , vol. 44, # 4 p. 541 - 546
反应条件
{(Pd{Fe(.eta.5-C5H5)(.eta.5-C5H3C(CH3)=NC6H4CH3-4)}(.mu.-Cl))2}; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in acetonitrile
T=110°C; 16 h; Inert atmosphere; Reagent/catalyst;
参考文献
Hu, Hao; Yang, Fan; Wu, Yangjie
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10506 - 10511
反应条件
air; potassium tert-butylate in N,N-dimethyl-formamide
1.5 h; Ambient temperature;
参考文献
Akiyama, Shuzo; Tajima, Kunihiko; Nakatsuji, Shin'ichi; Nakashima, Kenichiro; Abiru, Kazuko; Watanabe, Miwa
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 7 p. 2043 - 2052
反应条件
potassium tert-butylate in tetrahydrofuran
3 h; Ambient temperature;
参考文献
Kondo, Koichi; Fujitani, Takumi; Ohnishi, Noriaki
Journal of Materials Chemistry, 1997 , vol. 7, # 3 p. 429 - 433
反应条件
air; potassium tert-butylate in N,N-dimethyl-formamide
1.5 h; Ambient temperature;
参考文献
Akiyama, Shuzo; Tajima, Kunihiko; Nakatsuji, Shin'ichi; Nakashima, Kenichiro; Abiru, Kazuko; Watanabe, Miwa
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 7 p. 2043 - 2052
反应条件
1: 80 percent / NaOEt / ethanol; dimethylformamide / 3 h / Ambient temperature
2: 39 percent / t-BuOK, air / dimethylformamide / 1.5 h / Ambient temperature
View Scheme
参考文献
Akiyama, Shuzo; Tajima, Kunihiko; Nakatsuji, Shin'ichi; Nakashima, Kenichiro; Abiru, Kazuko; Watanabe, Miwa
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 7 p. 2043 - 2052
反应条件
1: 80 percent / NaOEt / ethanol; dimethylformamide / 3 h / Ambient temperature
2: 39 percent / t-BuOK, air / dimethylformamide / 1.5 h / Ambient temperature
View Scheme
参考文献
Akiyama, Shuzo; Tajima, Kunihiko; Nakatsuji, Shin'ichi; Nakashima, Kenichiro; Abiru, Kazuko; Watanabe, Miwa
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 7 p. 2043 - 2052
