2-氯-N-乙基-N-苯基乙酰胺合成路线 （共 7 条）
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran T=0°C;
参考文献
Pasquinucci, Lorella; Prezzavento, Orazio; Marrazzo, Agostino; Amata, Emanuele; Ronsisvalle, Simone; Georgoussi, Zafiroula; Fourla, Danai-Dionysia; Scoto, Giovanna M.; Parenti, Carmela; Arico, Giuseppina; Ronsisvalle, Giuseppe
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 14 p. 4975 - 4982
反应条件
trimethylamine borane in xylene 7 h; Heating;
参考文献
Trapani, Giuseppe; Reho, Antonia; Latrofa, Andrea
Synthesis, 1983 , # 12 p. 1013 - 1014
反应条件
nickel(II) salen; [Me4N][BF4] in N,N-dimethyl-formamide Electrolysis;
参考文献
Pasciak, Erick M.; Sengupta, Arkajyoti; Mubarak, Mohammad S.; Raghavachari, Krishnan; Peters, Dennis G.
Electrochimica Acta, 2014 , vol. 127, p. 159 - 166
反应条件
1: AlCl3 / 160 - 170 °C
2: POCl3
View Scheme
参考文献
Benkli, Kadriye; Demirayak, Seref; Gundogdu-Karaburun, Nalan; Kiraz, Nuri; Iscan, Gokalp; Ucucu, Umit
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 1 p. 174 - 179
反应条件
1: nickel(II) salen; [Me4N][BF4] / N,N-dimethyl-formamide / |Electrolysis
2: potassium hydroxide / water; ethyl acetate / 1 h / 0 °C
View Scheme
参考文献
Pasciak, Erick M.; Sengupta, Arkajyoti; Mubarak, Mohammad S.; Raghavachari, Krishnan; Peters, Dennis G.
Electrochimica Acta, 2014 , vol. 127, p. 159 - 166
反应条件
nickel(II) salen; [Me4N][BF4] in N,N-dimethyl-formamide
Electrolysis;
参考文献
Pasciak, Erick M.; Sengupta, Arkajyoti; Mubarak, Mohammad S.; Raghavachari, Krishnan; Peters, Dennis G.
Electrochimica Acta, 2014 , vol. 127, p. 159 - 166
反应条件
palladium diacetate; triethylamine; biphenyl-2-yl-di-tert-butyl-phosphane in toluene
T=80°C; 3 h;
参考文献
Hennessy, Edward J.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2003 , vol. 125, # 40 p. 12084 - 12085
