2-氯-n-(2,4,6-三甲基-苯基)-乙酰胺合成路线 （共 7 条）
反应条件
potassium carbonate in acetonitrile
参考文献
Paczal, Attila; Benyei, Attila C.; Kotschy, Andras
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5969 - 5979
反应条件
1: aq.-ethanolic sulfuric acid / bei der elektrochemischen Reduktion 2: sodium acetate; aqueous acetic acid View Scheme
参考文献
Loefgren
Arkiv foer Kemi, 1946 , vol. 22A, # 18 p. 11
参考文献
Loefgren
Arkiv foer Kemi, 1946 , vol. 22A, # 18 p. 11
反应条件
in ethanol; water
T=90 - 95°C; 5 h;
参考文献
Mikiciuk-Olasik, Elzbieta; Wojewoda, Emilia; Bilichowski, Ireneusz; Witczak, Malgorzata; Karwowski, Boleslaw; Wagrowska-Danilewicz, Malgorzata; Stasikowska, Olga
Acta Poloniae Pharmaceutica - Drug Research, 2010 , vol. 67, # 2 p. 119 - 127
反应条件
in butanone
T=80 - 90°C; 10 h;
参考文献
Stankyavichene, L. M. M.; Puzanov, G. I.; Stankyavichyus, A. P.; Gendenshtein, E. I.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 5 p. 341 - 344
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 5 p. 554 - 558
反应条件
in acetone
T=70 - 90°C; 15 h;
参考文献
Zhukauskaite, L. N.; Tsybusov, A. P.; Gendenshtein, E. I.; Stankevichyus, A. P.; Tseplene, V. S.; Lubas, A. A.
Pharmaceutical Chemistry Journal, 1981 , vol. 15, # 6 p. 391 - 396
Khimiko-Farmatsevticheskii Zhurnal, 1981 , vol. 15, # 6 p. 43 - 48
反应条件
1: 92 percent / NaN3 / methanol / Heating
2: 78 percent / LiAlH4 / tetrahydrofuran / Heating
View Scheme
参考文献
Paczal, Attila; Benyei, Attila C.; Kotschy, Andras
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5969 - 5979
