2-乙酰氧基乙基膦酸二甲酯合成路线 （共 8 条）
反应条件
1: dimethyl hydrogen phosphite With di-tert-butyl peroxide T=130°C; P=1500.12 Torr; 0.25 h; 2: vinyl acetate With di-tert-butyl peroxide T=130 - 150°C; 4 h;
参考文献
Boutevin; Hervaud; Jeanmaire; Boulahna; Elasri
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 174, p. 1 - 14
反应条件
2-tert-butylperoxy-2-methylpentan-4-one T=135 - 140°C; 0.5 h;
参考文献
Brel', A. K.; Tyurenkov, I. N.; Strel'tsova, G. V.; Matyukhova, N. P.; Nazarenko, V. N.; Agarkova, N. S.
Pharmaceutical Chemistry Journal, 1988 , vol. 22, # 2 p. 118 - 120
Khimiko-Farmatsevticheskii Zhurnal, 1988 , vol. 22, # 2 p. 167 - 170
反应条件
potassium hydroxide in methanol; water T=60°C; 24 h;
参考文献
Iftene, Fadela; David, Ghislain; Boutevin, Bernard; Auvergne, Remi; Alaaeddine, Ali; Meghabar, Rachid
Journal of Polymer Science, Part A: Polymer Chemistry, 2012 , vol. 50, # 12 p. 2432 - 2443
反应条件
hydrogenchloride in water T=100 - 115°C; 14 h;
参考文献
Kleiner, Hanss-Jerg; Schumann, Christian
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 363 - 370
反应条件
hydrogenchloride in water T=100°C; 11 h;
参考文献
Kleiner, Hanss-Jerg; Schumann, Christian
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 363 - 370
反应条件
hydrogenchloride in water T=100°C; 11 h;
参考文献
Kleiner, Hanss-Jerg; Schumann, Christian
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 363 - 370
反应条件
triphenylphosphine in water
参考文献
Zotov; Tuzhikov; Khokhlova
Russian Journal of Applied Chemistry, 2012 , vol. 85, # 4 p. 639 - 643
反应条件
hydrogenchloride in water T=100°C; 11 h;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 13, p. 363 - 370
