3-丙-2-烯基-1,3-噻唑烷-2,4-二酮合成路线 （共 13 条）
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 7 h; Inert atmosphere; regioselective reaction;
参考文献
Dhara, Kalyan; Paladhi, Sushovan; Midya, Ganesh Chandra; Dash, Jyotirmayee
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 10 p. 3801 - 3807
反应条件
in water
T=85°C; 1 h;
参考文献
Levshin, I. B.; Grigor'eva, I. V.; Tsurkan, A. A.; Tarasyavichus, E. L.; V'yunov, K. A.; Ginak, A. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 3 p. 277 - 279
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 3 p. 336 - 338
反应条件
in N,N-dimethyl-formamide
Reflux;
参考文献
Nitsche, Christoph; Schreier, Verena N.; Behnam, Mira A. M.; Kumar, Anil; Bartenschlager, Ralf; Klein, Christian D.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 21 p. 8389 - 8403
反应条件
hydrogenchloride
0.25 h; Heating;
参考文献
Levshin, I. B.; Grigor'eva, I. V.; Tsurkan, A. A.; Tarasyavichus, E. L.; V'yunov, K. A.; Ginak, A. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 3 p. 277 - 279
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 3 p. 336 - 338
反应条件
in ethanol
T=160 - 170°C;
参考文献
Vladzimirskaya,E.V.
J. Gen. Chem. USSR (Engl. Transl.), 1962 , vol. 32, p. 2019 - 2022,2000 - 2002
反应条件
acetic acid
3 h; Heating;
参考文献
Levshin, I. B.; Chistyakov, V. V.; Pol'shakov, V. I.; Sheinker, Yu. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, p. 910 - 914
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 8 p. 1135 - 1140
反应条件
hydrogenchloride in various solvent(s)
8 h; Heating;
参考文献
Sabu, M.; Garnaik, B. K.; Behera, Rajani K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 779 - 781
反应条件
hydrogenchloride in various solvent(s)
8 h; Heating;
参考文献
Sabu, M.; Garnaik, B. K.; Behera, Rajani K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 779 - 781
反应条件
hydrogenchloride in various solvent(s)
8 h; Heating;
参考文献
Sabu, M.; Garnaik, B. K.; Behera, Rajani K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 779 - 781
反应条件
hydrogenchloride in various solvent(s)
8 h; Heating;
参考文献
Sabu, M.; Garnaik, B. K.; Behera, Rajani K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 779 - 781
