7-硝基-9H-芴-2-甲腈合成路线 （共 7 条）
参考文献
University of Central Florida Research Foundation, Inc.
Patent: US8232303 B1, 2012 ;
Location in patent: Page/Page column 3 ;
反应条件
in N,N-dimethyl-formamide
1.5 h; Heating;
参考文献
Yao, Sheng; Schafer-Hales, Katherine J.; Belfield, Kevin D.
Organic Letters, 2007 , vol. 9, # 26 p. 5645 - 5648
反应条件
1: 1.) I2, 2.) H2SO4, NaNO2 / 1.) AcOH, RT, 10 min, 2.) reflux, 30 min
2: 30 percent / dimethylformamide / 4 h / Heating
View Scheme
参考文献
Marhevka, Virginia C.; Ebner, Nancy A.; Sehon, Russell D.; Hanna, Patrick E.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 1 p. 18 - 24
反应条件
in N,N-dimethyl-formamide
4 h; Heating;
参考文献
Marhevka, Virginia C.; Ebner, Nancy A.; Sehon, Russell D.; Hanna, Patrick E.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 1 p. 18 - 24
反应条件
1: (nitration)
2: 2-methyl-propan-2-ol; H2O / Irradiation
View Scheme
参考文献
Vink,J.A.J. et al.
Tetrahedron, 1972 , vol. 28, p. 5081 - 5087
反应条件
in water; tert-butyl alcohol
Irradiation;
参考文献
Vink,J.A.J. et al.
Tetrahedron, 1972 , vol. 28, p. 5081 - 5087
参考文献
Hayashi; Ishikawa
Yuki Gosei Kagaku Kyokaishi, 1955 , vol. 13, p. 171,173
Chem.Abstr., 1957 , p. 1920
