2-(2,4-二氟苯基)吡啶合成路线 （共 7 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in tetrahydrofuran T=70°C; Suzuki coupling; 24 h;
参考文献
You, Youngmin; Park, Soo Young
Journal of the American Chemical Society, 2005 , vol. 127, # 36 p. 12438 - 12439
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=70°C; 24 h;
参考文献
Chae, Hyun Sik; Ohmori, Yutaka; Froehlich, Jesse; Li, Sheng; Mochizuki, Amane
Patent: US2012/305895 A1, 2012 ;
Location in patent: Page/Page column 36 ;
反应条件
Suzuki coupling; Inert atmosphere;
参考文献
Park, Hye Rim; Kim, Bo Young; Kim, Young Kwan; Ha, Yunkyoung
Journal of Nanoscience and Nanotechnology, 2012 , vol. 12, # 7 p. 5613 - 5618
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=120°C; 72 h;
参考文献
Takizawa, Shin-Ya; Echizen, Hidenori; Nishida, Jun-Ichi; Tsuzuki, Toshimitsu; Tokito, Shizuo; Yamashita, Yoshiro
Chemistry Letters, 2006 , vol. 35, # 7 p. 748 - 749
反应条件
1.1: tetrahydrofuran / 5 h / -60 °C 1.2: 0 °C / pH 1 / Inert atmosphere 2.1: potassium carbonate / tetraphenyl-phosphine-palladium / tetrahydrofuran / 4 h / 61 °C / Inert atmosphere View Scheme
参考文献
Cai, Lifei; Zhao, Hongyu; Cai, Changquan
Patent: US2012/309971 A1, 2012 ;
反应条件
1: water; 2-ethoxy-ethanol 2: Na2CO3 / not given View Scheme
参考文献
You, Youngmin; Park, Soo Young
Journal of the American Chemical Society, 2005 , vol. 127, # 36 p. 12438 - 12439
反应条件
triethylsilane; 1,10-phenanthroline; NiII chloride hexahydrate; zinc in N,N-dimethyl-formamide T=100°C; 8 h; Sealed tube; regioselective reaction;
参考文献
He, Yi; Chen, Zhao; He, Chun-Yang; Zhang, Xingang
Chinese Journal of Chemistry, 2013 , vol. 31, # 7 p. 873 - 877
