6-氧代-5H-菲啶-3-羧酸合成路线 （共 5 条）
反应条件
1: Cu / 8 h / 200 °C
2: NH2NH2; Raney nickel / methanol
3: 1 N aq. NaOH
View Scheme
参考文献
Li, Jia-He; Serdyuk, Larisa; Ferraris, Dana V.; Xiao, Ge; Tays, Kevin L.; Kletzly, Paul W.; Li, Weixing; Lautar, Susan; Zhang, Jie; Kalish, Vincent J.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1687 - 1690
反应条件
1: Cu / 8 h / 200 °C
2: NH2NH2; Raney nickel / methanol
3: 1 N aq. NaOH
View Scheme
参考文献
Li, Jia-He; Serdyuk, Larisa; Ferraris, Dana V.; Xiao, Ge; Tays, Kevin L.; Kletzly, Paul W.; Li, Weixing; Lautar, Susan; Zhang, Jie; Kalish, Vincent J.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1687 - 1690
反应条件
1: NH2NH2; Raney nickel / methanol
2: 1 N aq. NaOH
View Scheme
参考文献
Li, Jia-He; Serdyuk, Larisa; Ferraris, Dana V.; Xiao, Ge; Tays, Kevin L.; Kletzly, Paul W.; Li, Weixing; Lautar, Susan; Zhang, Jie; Kalish, Vincent J.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1687 - 1690
反应条件
sodium azide; sulfuric acid in chloroform
Addition; rearrangement; Schmidt reaction; substitution; 15 h; Heating; Title compound not separated from byproducts.;
参考文献
Woodroofe, Carolyn C.; Zhong, Boyu; Lu, Xingliang; Silverman, Richard B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 2000 , # 1 p. 55 - 60
参考文献
Li, Jia-He; Serdyuk, Larisa; Ferraris, Dana V.; Xiao, Ge; Tays, Kevin L.; Kletzly, Paul W.; Li, Weixing; Lautar, Susan; Zhang, Jie; Kalish, Vincent J.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1687 - 1690
