3-氯-3-(4-甲基苯基)-3H-双吖丙啶合成路线 （共 5 条）
反应条件
Na(1+) cation-exchanged Y zeolite T=80°C; 48 h;
参考文献
Journal of the American Chemical Society, , vol. 128, # 46 p. 14836 - 14844
反应条件
in benzene T=0°C; Irradiation;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 16 p. 1090 - 1091
反应条件
1: 12 percent / NaOCl / H2O; diethyl ether / 0.08 h / cooling
2: 95 percent / t-BuOCl / CH2Cl2 / 24 h / 0 °C
3: LiBr / acetonitrile / 0.17 h / 20 °C
View Scheme
参考文献
Martinu, Tomas; Dailey, William P.
Journal of Organic Chemistry, 2006 , vol. 71, # 13 p. 5012 - 5015
反应条件
1: 95 percent / t-BuOCl / CH2Cl2 / 24 h / 0 °C
2: LiBr / acetonitrile / 0.17 h / 20 °C
View Scheme
参考文献
Martinu, Tomas; Dailey, William P.
Journal of Organic Chemistry, 2006 , vol. 71, # 13 p. 5012 - 5015
反应条件
sodium azide in dimethylsulfoxide-d6
Ambient temperatureIrradiationrelative rate; Mechanism;
参考文献
Creary, Xavier
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7700 - 7708
