3-(4-甲基苯基)-2-硫酮-1,3-噻唑啉-4-酮合成路线 (共 7 条)
反应条件
in 1,4-dioxane; methanol T=90°C; 0.416667 h;
参考文献
Omar, Mohamed T.; Shaban, Mohamed E.; El-Aasar, Nadia K.; Saied, Khaled F.
Helvetica Chimica Acta, 2008 , vol. 91, # 8 p. 1461 - 1470
反应条件
in water
2.5 h; Reflux;
参考文献
The Johns Hopkins University; Southern Methodist University; Biehl, Edward R.; Kamila, Sukanta; Dawson, Ted M.
Patent: US2013/253021 A1, 2013 ;
Location in patent: Paragraph 0055; 0056 ;
反应条件
in ammonium hydroxide
Hantzsch's cyclization;
参考文献
Kasmi-Mir, Souad; Djafri, Ayada; Hamelin, Jack; Paquin, Ludovic; Bazureau, Jean Pierre; Rahmouni, Mustapha
Synthetic Communications, 2007 , vol. 37, # 22 p. 4017 - 4034
反应条件
ammonium hydroxide; sodium hydroxide
参考文献
Taniyama et al.
Yakugaku Zasshi, 1959 , vol. 79, p. 1462,1464, 1465
Chem.Abstr., 1960 , p. 6689
参考文献
Andreasch; Zipser
Monatshefte fuer Chemie, 1905 , vol. 26, p. 1193
反应条件
(i) aq. Me3N, (ii) Ac2O; Multistep reaction;
参考文献
Garraway,J.L.
Journal of the Chemical Society, 1961 , p. 3733 - 3735
参考文献
Pujari; Rout
Journal of Scientific and Industrial Research, 1955 , vol. 14 B, p. 398