N-(4-甲基苄基)-n-丙胺合成路线 （共 7 条）
反应条件
[(C5Me5)IrI2]2 in water
T=115°C; 10 h; Inert atmosphere;
参考文献
Saidi, Ourida; Blacker, A. John; Farah, Mohamed M.; Marsden, Stephen P.; Williams, Jonathan M. J.
Chemical Communications, 2010 , vol. 46, # 9 p. 1541 - 1543
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Orito, Kazuhiko; Horibata, Akiyoshi; Nakamura, Takatoshi; Ushito, Harumi; Nagasaki, Hideo; Yuguchi, Motoki; Yamashita, Satoshi; Tokuda, Masao
Journal of the American Chemical Society, 2004 , vol. 126, # 44 p. 14342 - 14343
反应条件
1: 72 percent / CH2Cl2 / 48 h / Ambient temperature
2: 1.) Bu3SnH, AIBN; 2.) NaBH4 / 1.) cyclohexane, 2.5 h, reflux; 2.) DMF/cyclohexane, r.t., 60 min
View Scheme
参考文献
Bowman, W. Russell; Clark, David N.; Marmon, Robert J.
Tetrahedron, 1994 , vol. 50, # 4 p. 1275 - 1294
反应条件
sodium tetrahydroborate; 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride
1.) cyclohexane, 2.5 h, reflux; 2.) DMF/cyclohexane, r.t., 60 min; Yield given. Multistep reaction;
参考文献
Bowman, W. Russell; Clark, David N.; Marmon, Robert J.
Tetrahedron, 1994 , vol. 50, # 4 p. 1275 - 1294
反应条件
1: p-TsOH / toluene / Heating
2: NaBH4 / methanol / Heating
3: 72 percent / CH2Cl2 / 48 h / Ambient temperature
4: 1.) Bu3SnH, AIBN; 2.) NaBH4 / 1.) cyclohexane, 2.5 h, reflux; 2.) DMF/cyclohexane, r.t., 60 min
View Scheme
参考文献
Bowman, W. Russell; Clark, David N.; Marmon, Robert J.
Tetrahedron, 1994 , vol. 50, # 4 p. 1275 - 1294
反应条件
1: NaBH4 / methanol / Heating
2: 72 percent / CH2Cl2 / 48 h / Ambient temperature
3: 1.) Bu3SnH, AIBN; 2.) NaBH4 / 1.) cyclohexane, 2.5 h, reflux; 2.) DMF/cyclohexane, r.t., 60 min
View Scheme
参考文献
Bowman, W. Russell; Clark, David N.; Marmon, Robert J.
Tetrahedron, 1994 , vol. 50, # 4 p. 1275 - 1294
参考文献
Bowman, W. Russell; Clark, David N.; Marmon, Robert J.
Tetrahedron, 1994 , vol. 50, # 4 p. 1275 - 1294
