1-(3,5-二甲氧基苯基)庚烷-1-酮合成路线 （共 12 条）
反应条件
1.1: oxalyl chloride / CH2Cl2; dimethylformamide / 1 h / Heating
2.1: 11.86 g / pyridine / CH2Cl2 / 0 - 20 °C
3.1: Mg / tetrahydrofuran / 0.5 h / 20 °C
3.2: 90 percent / tetrahydrofuran / 1.5 h / 0 °C
View Scheme
参考文献
Harrington, Paul E.; Stergiades, Ioanna A.; Erickson, Joy; Makriyannis, Alexandros; Tius, Marcus A.
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6576 - 6582
反应条件
1.1: 11.86 g / pyridine / CH2Cl2 / 0 - 20 °C
2.1: Mg / tetrahydrofuran / 0.5 h / 20 °C
2.2: 90 percent / tetrahydrofuran / 1.5 h / 0 °C
View Scheme
参考文献
Harrington, Paul E.; Stergiades, Ioanna A.; Erickson, Joy; Makriyannis, Alexandros; Tius, Marcus A.
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6576 - 6582
