4-氯-N-(4-氯苯基)苯甲酰胺合成路线 （共 22 条）
反应条件
triethylamine in acetonitrile
5 h; Heating;
参考文献
Rebelo, Ricardo Andrade; Rezende, Marcos Caroli; Nome, Faruk; Zucco, Cesar
Synthetic Communications, 1987 , vol. 17, # 14 p. 1741 - 1748
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine; triethyl phosphite
T=120 - 130°C; 8 h;
参考文献
Chiriac, Constantin I.; Tanasa, Fulga; Onciu, Marioara
Revue Roumaine de Chimie, 2006 , vol. 51, # 4 p. 269 - 272
反应条件
1: CH2Cl2 / Ambient temperature
2: 1.) CF3SO3Me, 2.) N-methylmorpholine / 1.) ClCH2CH2Cl, RT, 5 min, 2.) ClCH2CH2Cl, 20 deg C, 4 h
View Scheme
参考文献
Ulibarri, Gerardo; Choret, Nadege; Bigg, Dennis C. H.
Synthesis, 1996 , # 11 p. 1286 - 1288
反应条件
di-tert-butyl peroxide; chlorobenzene
T=110°C; 48 h; Further byproducts given;
参考文献
Leardini, Rino; Tundo, Antonio; Zanardi, Giuseppe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3164 - 3167
反应条件
4-methyl-morpholine; methyl trifluoromethanesulfonate
1.) ClCH2CH2Cl, RT, 5 min, 2.) ClCH2CH2Cl, 20 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Ulibarri, Gerardo; Choret, Nadege; Bigg, Dennis C. H.
Synthesis, 1996 , # 11 p. 1286 - 1288
反应条件
aluminium trichloride
参考文献
Effenberger,F.; Gleiter,R.
Chemische Berichte, 1964 , vol. 97, p. 472 - 479
反应条件
9,10-dihydro-anthracene; water
T=356.85°C; 3 h; Kinetics;
参考文献
Mulder, Peter; Arends, Isabel W. C. E.; Santoro, Danilo; Korth, Hans-Gert
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4247 - 4257
反应条件
anschliessend mit 4-Chlor-benzaldehyd und Pyridin;
参考文献
Tetjuewa; Petjunin
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 739,740; engl.Ausg.S.719
反应条件
in methanol
T=55°C; Rate constant;
参考文献
Lee, Ikchoon; Shim, Chang Sub; Lee, Hai Whang
Journal of Chemical Research, Miniprint, 1992 , # 3 p. 769 - 793
反应条件
in methanol
T=55°C; Rate constant;
参考文献
Lee, Ikchoon; Shim, Chang Sub; Lee, Hai Whang
Journal of Chemical Research, Miniprint, 1992 , # 3 p. 769 - 793
