二(3-甲氧基苯基)甲酮合成路线 （共 15 条）
反应条件
1: diethyl ether / 20 °C
2: oxalyl chloride; DMSO; triethylamine / CH2Cl2 / 20 °C
View Scheme
参考文献
Mills, Nancy S.; Tirla, Cornelia; Benish, Michele A.; Rakowitz, Amber J.; Bebell, Lisa M.; Hurd, Caroline M. M.; Bria, Anna L. M.
Journal of Organic Chemistry, 2005 , vol. 70, # 26 p. 10709 - 10716
反应条件
magnesium
1) THF, 2) THF, r.t.; Yield given. Multistep reaction;
参考文献
Groundwater, Paul W.; Sharp, John T.
Tetrahedron, 1992 , vol. 48, # 37 p. 7951 - 7964
参考文献
Pohlmann
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 737,740
反应条件
1: (diphenylmethyl)trimethylsilane With n-butyllithium in tetrahydrofuran
T=20°C; 8 h;
2: bis-(3-methoxy-phenyl)-methanone in tetrahydrofuran
T=20°C; Peterson olefination; 24 h;
3: With sulfuric acid in dichloromethane
T=20°C; 16 h;
参考文献
Mills, Nancy S.; Tirla, Cornelia; Benish, Michele A.; Rakowitz, Amber J.; Bebell, Lisa M.; Hurd, Caroline M. M.; Bria, Anna L. M.
Journal of Organic Chemistry, 2005 , vol. 70, # 26 p. 10709 - 10716
参考文献
Melby et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 3816
