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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
39195-66-9
合成路线
（共 23 条）
1142173-50-9
→
反应条件
39195-66-9
反应条件
potassium carbonate in water T=110°C; 2 h; Microwave irradiationInert atmosphereGreen chemistry;
参考文献
Sun, Shi-Xin; Wang, Jun-Jie; Xu, Zi-Jun; Cao, Lu-Ya; Shi, Zi-Fa; Zhang, Hao-Li
Tetrahedron, 2014 , vol. 70, # 24 p. 3798 - 3806
873-73-4
对氯苯乙炔
+
533-58-4
2-碘苯酚
→
反应条件
39195-66-9
反应条件
sodium tetrachloropalladium (II); sodium lauryl sulfate; triethylamine in water T=100°C; Sonogashira coupling; 12 h;
参考文献
Saha, Debasree; Dey, Raju; Ranu, Brindaban C.
European Journal of Organic Chemistry, 2010 , # 31 p. 6067 - 6071
54008-77-4
2-溴-1-苯并呋喃
+
5575-51-9
→
反应条件
39195-66-9
+
2050-68-2
4,4'-二氯联苯
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in 1-methyl-pyrrolidin-2-one T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L.N.; Awasthi, Dheeraj K.; Talode, Jalindar B.
Tetrahedron Letters, 2012 , vol. 53, # 21 p. 2662 - 2666
14714-50-2
2-羟基苯乙腈
+
1679-18-1
4-氯苯硼酸
→
反应条件
39195-66-9
反应条件
[2,2']bipyridinyl; palladium diacetate; trifluoroacetic acid in tetrahydrofuran; water T=80°C; 36 h; Schlenk techniqueInert atmosphere;
参考文献
Wang, Xingyong; Wang, Xiaodong; Liu, Miaochang; Ding, Jinchang; Chen, Jiuxi; Wu, Huayue
Synthesis (Germany), 2013 , vol. 45, # 16 art. no. SS-2013-F0255-OP, p. 2241 - 2244
1276042-58-0
→
反应条件
39195-66-9
反应条件
triethylamine in tetrachloromethane Wittig reaction; Irradiation;
参考文献
Ghosh, Somnath; Das, Jhantu
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2423 - 2423
42224-51-1
→
反应条件
39195-66-9
反应条件
[bis(acetoxy)iodo]benzene in acetonitrile T=20°C; 2 h; Inert atmosphere;
参考文献
Singh, Fateh V.; Wirth, Thomas
Synthesis, 2012 , vol. 44, # 8 p. 1171 - 1177
14714-50-2
2-羟基苯乙腈
+
14752-66-0
对氯苯亚磺酸钠
→
反应条件
39195-66-9
反应条件
[2,2']bipyridinyl; para-nitrobenzenesulfonic acid; palladium diacetate in 2-methyl tetrahydrofuran; water T=80°C; 36 h; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Chen, Jiuxi; Li, Jianjun; Su, Weike
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 24 p. 4078 - 4083
14752-66-0
对氯苯亚磺酸钠
+
91703-34-3
→
反应条件
39195-66-9
反应条件
1: 2-(gem-dibromovinyl)phenol With tetrabutyl ammonium fluoride in N,N-dimethyl-formamide T=20°C; 4 h; Sealed tubeInert atmosphere; 2: p-chlorobenzenesulphinic acid sodium salt With copper diacetate; triethylamine; palladium dichloride in N,N-dimethyl-formamide T=110°C; 12 h; Sealed tubeInert atmosphere;
参考文献
Chen, Wei; Li, Pinhua; Miao, Tao; Meng, Ling-Guo; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 3 p. 420 - 424
14714-50-2
2-羟基苯乙腈
→
反应条件
39195-66-9
反应条件
[2,2']bipyridinyl; palladium (II) trifluoroacetate; water; trifluoroacetic acid in tetrahydrofuran T=80°C; 36 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Xingyong; Liu, Miaochang; Xu, Long; Wang, Qingzong; Chen, Jiuxi; Ding, Jinchang; Wu, Huayue
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5273 - 5281
52803-59-5
→
反应条件
39195-66-9
反应条件
aluminum oxide; alkali metal fluoride in N,N-dimethyl-formamide T=153°C; 4 h;
参考文献
Hellwinkel; Goke
Synthesis, 1995 , # 9 p. 1135 - 1141
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