反应条件
1: sodium hydride / N,N-dimethyl-formamide / 20 °C / |Inert atmosphere; |Cooling with ice
2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 50 °C / |Inert atmosphere
3: hydrogenchloride / methanol; water / |Reflux; |Inert atmosphere
4: potassium carbonate / water / 2 h / 110 °C / |Microwave irradiation; |Inert atmosphere; |Green chemistry
View Scheme
参考文献
Sun, Shi-Xin; Wang, Jun-Jie; Xu, Zi-Jun; Cao, Lu-Ya; Shi, Zi-Fa; Zhang, Hao-Li
Tetrahedron, 2014 , vol. 70, # 24 p. 3798 - 3806
