2-氯代五氟-1,3-丁二烯合成路线 （共 3 条）
反应条件
potassium hydroxide; paraffin oil
参考文献
Park et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1661,1662
反应条件
vanadium(V) fluoride in monofluoro-trichloromethane T=-20°C; 0.333333 h;
参考文献
Petrov, V. A.; Bardin, V. V.; Furin, G. G.; Avramenko, A. A.; Galakhov, M. V.; et al.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 37 - 41
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 1 p. 43 - 48
反应条件
sulfuric acid; ClSO2F (sulfuryl chloride fluoride); SbF5
1) -10 deg C, 2) heating; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chepick, S. D.; Belen'kii, G. G.; Petrov, V. A.; German, L. S.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 3 p. 223 - 226
