iron(II) chloride in tetrahydrofuran reaction of 2 mol C2H5MgBr and 1 mol C6F6 at 0°C in presence of FeCl2 (molar fraction 0.02) within 0.5 hours;;
参考文献
Respess, W. L.; Tamborski, C.
Journal of Organometallic Chemistry, 1969 , vol. 18, p. 263 - 274
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
in tetrahydrofuran addition of a solution of C2H4Br2 in THF drop by drop to a mixture of Mg and C6F6/THF (mol ratio C2H4Br2/C6F6 = 2/1) within 0.75 hours, cooling with ice water;;
参考文献
Respes et al.
Journal of Organometallic Chemistry, 1969 , vol. 19, p. 191
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
in tetrahydrofuran addition of a solution of C2H5Br in THF drop by drop to a mixture of Mg and C6F6/THF (mol ratio C2H5Br/C6F6 = 1/1) within 0.75 hours, cooling with ice water;;
参考文献
Respes et al.
Journal of Organometallic Chemistry, 1969 , vol. 19, p. 191
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67