2,4,6-三甲基-1,3-二氟苯合成路线 （共 8 条）
反应条件
1: hydrogen fluoride; sodium nitrate 2: iron 3: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
XeF2; hydrogen fluoride in dichloromethane
T=25°C; 0.333333 h;
参考文献
Stavber, Stojan; Zupan, Marko
Journal of Organic Chemistry, 1983 , vol. 48, # 13 p. 2223 - 2226
反应条件
hydrogenchloride; sodium tetrafluoroborate; sodium nitrite
Erhitzen des Reaktionsprodukts;
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: iron
2: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts
View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: aqueous hydrochloric acid; sodium nitrite; aqueous sodium-tetrafluoroborate / Erhitzen des Reaktionsprodukts
2: iron
3: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts
View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide
T=105°C; 1.67 h;
参考文献
Andreev; Borodkin; Shubin
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 10 p. 1468 - 1473
反应条件
1: AlCl3
2: aqueous NaBrO
3: AgNO3; ethanol / anschliessend Erwaermen mit wss. NaOH
View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: hydrogen fluoride; sodium nitrate
2: iron
3: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts
4: tetrachloromethane; chlorine / Licht einer 200 W-Lampe
View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
