1H-吲哚-1-羧酸甲酯合成路线 （共 34 条）
反应条件
T=700°C; Yield given. Title compound not separated from byproducts;
参考文献
Qiao; Meutermans; Wong; Traubel; Wentrup
Journal of the American Chemical Society, 1996 , vol. 118, # 16 p. 3852 - 3861
反应条件
1: With tri-isopropoxy-borane; lithium diisopropyl amide in tetrahydrofuran T=0 - 5°C; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; water
参考文献
Tetrahedron, , vol. 65, # 34 p. 6877 - 6881
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane T=-10 - -5°C; 3.5 h;
参考文献
Organic Process Research and Development, , vol. 11, # 6 p. 1051 - 1054
反应条件
T=700°C; Yield given. Title compound not separated from byproducts;
参考文献
Qiao; Meutermans; Wong; Traubel; Wentrup
Journal of the American Chemical Society, 1996 , vol. 118, # 16 p. 3852 - 3861
反应条件
sodium hydride in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Chelucci, Giorgio; Pinna, Gerard A.; Pinna, Giansalvo
European Journal of Organic Chemistry, 2014 , vol. 2014, # 18 p. 3802 - 3807
反应条件
triethylamine; triphenylphosphine; palladium diacetate in acetonitrile
T=110 - 115°C; 13 h;
参考文献
Somei; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 11 p. 3145 - 3157
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
T=20°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Heller, Stephen T.; Schultz, Erica E.; Sarpong, Richmond
Angewandte Chemie - International Edition, 2012 , vol. 51, # 33 p. 8304 - 8308
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide
T=94°C; 0.166667 h;
参考文献
Shieh, Wen-Chung; Dell, Steven; Bach, Andrew; Repic, Oljan; Blacklock, Thomas J.
Journal of Organic Chemistry, 2003 , vol. 68, # 5 p. 1954 - 1957
反应条件
1: indole; carbon dioxide With lithium tert-butylate in N,N-dimethyl-formamide
T=20°C; 15 h;
2: methyl iodide in N,N-dimethyl-formamide
参考文献
Yoo, Woo-Jin; Capdevila, Montse Guiteras; Du, Xiangwei; Kobayashi, Shu
Organic Letters, 2012 , vol. 14, # 20 p. 5326 - 5329,4
反应条件
toluene-4-sulfonic acid in ethanol
13 h; Ambient temperature;
参考文献
Samizu, Kiyohiro; Ogasawara, Kunio
Heterocycles, 1995 , vol. 41, # 8 p. 1627 - 1630
