1,1-二苯基-2-丙炔-1-醇合成路线 (共 64 条)
反应条件
toluene-4-sulfonic acid in acetonitrile 12 h; Ambient temperature;
参考文献
Chamontin, Karine; Lokshin, Vladimir; Rossollin, Valerie; Samat, Andre; Guglielmetti, Robert
Tetrahedron, 1999 , vol. 55, # 18 p. 5821 - 5830
反应条件
toluene-4-sulfonic acid in dichloromethane Ambient temperature;
参考文献
Chamontin, Karine; Lokshin, Vladimir; Rossollin, Valerie; Samat, Andre; Guglielmetti, Robert
Tetrahedron, 1999 , vol. 55, # 18 p. 5821 - 5830
反应条件
1: 90 percent / pTSA / CH2Cl2 / Ambient temperature 2: 1.) n-BuLi / 1.) hexane, Et2O, 0 deg C, 1 h, 2.) 1 h View Scheme
参考文献
Chamontin, Karine; Lokshin, Vladimir; Rossollin, Valerie; Samat, Andre; Guglielmetti, Robert
Tetrahedron, 1999 , vol. 55, # 18 p. 5821 - 5830
反应条件
pyridine; copper diacetate in methanol T=60°C; 10 h;
参考文献
Zouev; Cao, Den-Ke; Sreevidya; Telzhensky; Botoshansky; Kaftory
CrystEngComm, 2011 , vol. 13, # 13 p. 4376 - 4381
反应条件
methanol; ethylamine; copper(l) chloride
参考文献
Chodkiewicz
Annales de Chimie (Cachan, France), 1957 , vol. <13> 2, p. 819,861, 862
反应条件
diethyl ether anschliessend Einleiten von Kohlendioxid;
参考文献
Sal'kind; Michant'ew
Zhurnal Obshchei Khimii, 1941 , vol. 11, p. 92,97, 98
Chem. Zentralbl., 1941 , vol. 112, # II p. 1609
反应条件
1: diethyl ether / anschliessend Einleiten von Kohlendioxid 2: palladium; diethyl ether / Hydrogenation View Scheme
参考文献
Sal'kind; Michant'ew
Zhurnal Obshchei Khimii, 1941 , vol. 11, p. 92,97, 98
Chem. Zentralbl., 1941 , vol. 112, # II p. 1609
反应条件
1: 1,1-diphenyl-2-propyn-1-ol With potassium phosphate; palladium diacetate; triethylamine; triphenylphosphine in acetonitrile Sonogashira coupling; 0.5 h; Inert atmosphere; 2: iodobenzene in acetonitrile T=20°C; Sonogashira coupling; 12 h; Inert atmosphere;
参考文献
Braga, Daniele; Jaafari, Abdelhafid; Miozzo, Luciano; Moret, Massimo; Rizzato, Silvia; Papagni, Antonio; Yassar, Abderrahim
European Journal of Organic Chemistry, 2011 , # 22 p. 4160 - 4169
反应条件
silver hexafluoroantimonate; {1,3-bis[2,6-di(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}AuCl; water in methanol T=60°C;
参考文献
Ramon, Ruben S.; Marion, Nicolas; Nolan, Steven P.
Tetrahedron, 2009 , vol. 65, # 9 p. 1767 - 1773
反应条件
C44H40Cl2NPRuS2 T=90°C; Nicholas reaction;
参考文献
Costin, Stephen; Sedinkin, Sergey L.; Bauer, Eike B.
Tetrahedron Letters, 2009 , vol. 50, # 8 p. 922 - 925