1H,1H,2H,2H,3H,3H,4H,4H-全氟癸烷-1-醇合成路线 (共 7 条)
16083-68-45,5,6,6,7,7,8,8,9,9,10,10,10-十三氟-3-碘-1-癸醇
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反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in diethyl ether; toluene
T=20°C; 3 h;
参考文献
Luscombe, Christine K.; Proemmel, Steffen; Huck, Wilhelm T. S.; Holmes, Andrew B.; Fukushima, Hitoshi
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5505 - 5513
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
Reduction; 6 h;
参考文献
Tra Anh; Blancou; Commeyras
Journal of Fluorine Chemistry, 1999 , vol. 96, # 2 p. 167 - 174
反应条件
lithium aluminium tetrahydride in diethyl ether
T=40°C; Reduction; 12 h;
参考文献
Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889
反应条件
1: AIBN / 15 h / 90 °C
2: 6.9 g / LiAlH4 / tetrahydrofuran / 2 h
View Scheme
参考文献
Luscombe, Christine K.; Proemmel, Steffen; Huck, Wilhelm T. S.; Holmes, Andrew B.; Fukushima, Hitoshi
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5505 - 5513
反应条件
1: 3 h / 195 °C
2: LiAlH4 / diethyl ether / 12 h / 40 °C
View Scheme
参考文献
Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889
反应条件
1: K2CO3 / tetrahydrofuran / 24 h / 70 °C
2: KOH / ethanol / 80 °C
3: 3 h / 195 °C
4: LiAlH4 / diethyl ether / 12 h / 40 °C
View Scheme
参考文献
Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889
反应条件
1: KOH / ethanol / 80 °C
2: 3 h / 195 °C
3: LiAlH4 / diethyl ether / 12 h / 40 °C
View Scheme
参考文献
Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889