1: 2-propene-1-thiol With sodium ethanolate in ethanol T=0 - 20°C; 1 h; 2: sodium salt of the chloroacetic acid in ethanol 18 h; Reflux; 3: With hydrogenchloride; water in THFytetrahydrofuranethanol
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1: With potassium hydroxide in DMF (N,N-dimethyl-formamide) T=153°C; 4 - 5 h; 2: With hydrogenchloride in DMF (N,N-dimethyl-formamide); water pH=4.0 - 4.5;
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Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2973 - 2978